Synthesis [1-(4-acetylphenyl)-3-(2-methylphenyl)]triazene: NMR, Vibrational, X-ray Crystallography Characterization with HF/DFT Studies

Citations:

2

Abstract

1-(4-acetylphenyl)-3-(2-methylphenyl)]triazene (AMT) was synthesized by experimental methods, its chemical and spectrometric properties were studied by FT-IR, FT-Raman, 1 H-NMR, 13 C-NMR and X-ray single-crystal diffraction methods.The obtained results showed that this structure has orthorombic system with space group of pbca and eight molecules in unit cell.Its unit cell parameters comprise a=8.0...

View PDF

Keywords

Triazene

Dihedral angle

Chemistry

Chemical shift

Raman spectroscopy

Carbon-13 NMR

Molecule

Crystallography

Proton NMR

Molecular geometry

Bond length

X-ray crystallography

Physical chemistry

Computational chemistry

Crystal structure

Diffraction

Stereochemistry

Hydrogen bond

Organic chemistry

Physics

Optics

2018

Article

Open Access

Institution

Young Researchers and Elite Club, Shahr-E-Rey Branch, Islamic Azad University, Tehran, Iran

2-Y Citation Average

0.712

DOI

https://doi.org/10.21608/ejchem.2018.2176.1173

Language

en

Country

Iran, Islamic Republic Of

Synthesis [1-(4-acetylphenyl)-3-(2-methylphenyl)]triazene: NMR, Vibrational, X-ray Crystallography Characterization with HF/DFT Studies

Egyptian Journal of Chemistry

reza soleymani, Abolfazl Aghaei

Citations:

2

Abstract

1-(4-acetylphenyl)-3-(2-methylphenyl)]triazene (AMT) was synthesized by experimental methods, its chemical and spectrometric properties were studied by FT-IR, FT-Raman, 1 H-NMR, 13 C-NMR and X-ray single-crystal diffraction methods.The obtained results showed that this structure has orthorombic system with space group of pbca and eight molecules in unit cell.Its unit cell parameters comprise a=8.0...